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United States Environmental Protection Agency
ESB Laboratory -- Region 6: South Central
  Serving Louisiana, Arkansas, Oklahoma, New Mexico, Texas and 66 Tribes
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ANALYTICAL CAPABILITY INVENTORY

Turnaround Times - Routine turnaround time is 35 days. Contact the Region 6 Sample Control Center for quicker turnaround times.

Concentration Ranges - The Region 6 Environmental Laboratory does not routinely analyze % level samples, however % level analyses can be accommodated. Please contact the Region 6 Sample Control Center.

Region 6 Environmental Services Assistance Team (ESAT) - Region 6 ESAT assists with sample preparation activities and limited analytical support.

The SW-846 methods and other documents can now be viewed and/or printed using the Adobe Acrobat Reader. You may download the reader for free Exit EPA if you do not have Adobe Acrobat on your computer.

 

CORE CAPABILITIES

Chemistry

 Analyte/Group

Media

Technique

Method/Comments *

Concentration Range

Cr+6

water

colorimetric

7196A

low ppb to % level

Mercury

water

CVAA

245.1

low ppb to % level

Mercury

soil/sediment

CVAA

245.5

low ppm to % level

Mercury

fish tissue

CVAA

245.6

low PPM to % level

Metals

water

GFAA, ICP, ICP/MS

200.2, 3010A, 3015- 200.7, 200.8 (Ultra low level), 200.9, 6010, 6020, 7000 series

clean fume hood used for ultra low level work

ppb to % level

Metals

fish tissue

GFAA, ICP, ICP/MS

200.3(mod) - 200.7, 200.8(low level), 200.9

low PPM to % level

Metals

soil/sediment

GFAA, ICP

200.2, 3050, 3051 - 200.7, 200.9, 6010, 7000 series

low PPM to % level

Metals

oil, other

GFAA, ICP

3050, 3051, 200.7, 200.9/ microwave digestion used when necessary

low PPM to % level

Ignitability

water, oil

closed cup

1010, 1020

ambient to 100oC

Conductance

water

specific

120.1

1 Fmho and up

Hardness, total

water

titrimetric, EDTA

130.2

low PPM and up

pH

water

electrometric

150.1

1 - 13 STD units

Solids

water

residue(gravimetric)

160.1-160.5

low PPM and up

Oil & Grease

water

n-hexane ext., solid phase

1664

low PPM to % level

Turbidity

water

nephelometric

180.1

1 NTU and up

Inorganic ions

water

ionic chromatography

300.0

low PPM to % level

Alkalinity

water

titrimetric

310.1

low PPM and up

Analyte/Group

Media

Technique

Method/Comments

Concentration Range

Cyanide

water

colorimetric

335.2

low ppb to 2%

Cyanide

soil/sediment

colorimetric

335.2

low PPM to 2%

Nitrogen(ammonia)

water

colorimetric

350.1

low ppb

Nitrogen(Kjedahl total)

water

colorimetric

351.2

low ppb

Nitrogen(Kjedahl total)

soil/sediment

colorimetric

351.2

low PPM

Nitrogen (nitrate-nitrite)

water

colorimetric

353.2

low ppb

Phosphorus (total)

water

colorimetry

365.4

low ppb

Phosphorus (ortho)

water

colorimetry

365.1

low ppb

BOD/CBOD

water

DO probe

405.1

low PPM

Phenolics, total rec.

water

colorimetric

420.1

low ppb

VOA

soils/sediment/waste

GC/MS

8260

low - mid ppb to % level

VOA

air

GC/MS

TO-14/8260 (Summa cannisters/Tedlar Bags)

low ppb to % level

VOA

water

GC/MS

524.2

low ppb

VOA

water

GC/MS

624, 8260

low ppb to % level

BNA

water

GC/MS

525.2

low ppb

BNA

water

GC/MS

625, 8270

low ppb to % level

BNA

soil/sediment/waste

GC/MS

8270

mid ppb to % level

PNA

water

GC/MS

525.2

low ppb

PNA

water

GC/MS

8270

low ppb to % level

PNA

soil/sediment

GC/MS

8270

mid ppb to % level

Pest/PCB

water

GC/ECD, GC/MS

508, 525.2

Pest = low - mid ppt

PCB = ppt - low ppb

Pest/PCB

water

GC/ECD, GC/MS

608, 8081, 8082

Pest = low - mid ppt to % level

PCB =low - mid ppt to % level

Pest/PCB

soil/sediment/waste

GC/ECD, GC/MS

8081, 8082

low ppb to % level

Herbicide

water

GC/ECD

515.2

low ppb

Herbicide

water

GC/ECD

8151A

low ppb to % level

Herbicide

soil/sediment

GC/ECD

8151A

mid ppb - % level

EDB/DBCP/1,2,3-TCP

water

GC

504.1

low ppt

TCLP

soil/sediment/oil/ waste

Tumbler/Analytical Instrumentation

1311

Extraction Method

See Analytical Method for water or waste

 

Microbiology

 

 Analyte/group

Media

Technique

Concentration Range

Total coliform, fecal coliform, E-coli

water

Standard Method: 9221

ICFU

SPECIAL CAPABILITIES

Chemistry

 Analyte/group

Media

Technique

Method / Unique Factor

Concentration Range

Incidental PCBs

water, hazardous waste

GC/MS

680, homologue series

low ppb to % level

Pesticides/PCBs/BNAs

soil/sediment

GC, GC/MS, Microwave

Proposed method 3546

Pest/PCB = low ppb to % level

BNA = mid ppb to % level

Pesticides/PCBs/BNAs

soil/sediment

GC, GC/MS, Microwave

Abbreviated and modified proposed method 3546 (removed concentration step) /8081, 8270

Pest/PCB = low ppb to % level

BNA = mid ppb to % level

Pesticides/BNAs

water

GC/MS, PTV, microextraction

Abbreviated and modified method 3510, 8081, 8270, 608, 625

Pest = low ppt to % level

BNA = low ppt to % level

BNA w/microextraction = low ppb to % level

TOX/TX

water, soil/sediment, waste

microcoulometric

9020

low ppm to % level

Finger Print (pattern recognition)

high level waste, oil, fuel

GC, GC/MS

no EPA method, similar to 8082 (Arochlor Identification)

ppm to % level

Aquatic Biology

 Analyte/group

Media

Technique

Method

Biomonitoring

water

acute

fresh/marine

Biomonitoring

water

chronic

fresh/marine

Biomonitoring

soil/sediment

acute

fresh/marine

Biomonitoring

soil/sediment

chronic

fresh/marine

  

* Method References

  1. Methods For The Determination of Organic Compounds In Drinking Water Supplement III, EPA/600/R-95/131 August 1995
  2. Methods For The Determination of Inorganic Substances in Environmental Samples, EPA/600-R-93/100 August 1993
  3. 40 CFR Part 136
  4. Methods For The Determination of Metals in Environmental Samples Supplement I, EPA/600/R-94/111 May 1994
  5. Methods For Chemical Analysis of Water and Wastes EPA/600/4-79-020 Revised March 1983
  6. Test Methods For Evaluating Solid Waste Physical Chemical Methods SW846

 

 
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