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Lake Michigan Mass Balance
Lake Michigan Mass Balance
Methods Compendium
June 1997
About the Methods Compendium
Methods
| Volume 1 |
Volume 2 |
Volume 3 |
| Sample Collection
Techniques |
Organic and Mercury sample
Analysis Techiques |
Metals, Conventions, Radiochemistry, and
Biomonitoring Sample Techniques |
|
Air,
Water,
Sediment,
Plankton,
Fish |
Organic Analysis,
Mercury Analysis |
Metals,
Conventionals,
Radiochemistry,
Biomonitoring,
Shipboard Measurements |
(back to other methods)
Chapter 1: Air
| LMMB 001 |
Standard Operating Procedure for Air Sampling for Semivolatile Organic
Contaminants Using the Organics High-Volume Sampler (Sweet, C.) |
| LMMB 002 |
Standard Operating Procedure for Precipitation Sampling Using XAD-2 and
MIC Collectors (Sweet, C.) |
| LMMB 003 |
Standard Operating Procedure for Air Sampling for Metals Using the
Dichotomous Sampler (Sweet, C.) |
| LMMB 004 |
Standard Operating Procedure for Sampling Trace Metals in Precipitation
Using Modified Aerochem Collectors (Vermette, S. and Sweet, C.) |
| LMMB 005 |
Metals Cleaning Procedures for Teflon Bottles and Rigid HDPE (Vermette, S.
and Sweet, C.) |
| LMMB 006 |
Standard Operating Procedure for Sampling of Vapor Phase Mercury (Keeler,
G. and Landis, M.) |
| LMMB 007 |
Standard Operating Procedure for Sampling of Mercury in Precipitation
(Keeler, G and Landis, M.) |
| LMMB 008 |
Standard Operating Procedure for Sampling of Particulate Phase Mercury
(Keeler, G. and Landis, M.) |
| LMMB 009 |
Standard Operating Procedure for Dry Deposition Sampling: Dry Deposition
of Atmospheric Particles (Paode, R. and Holsen, T.) |
Chapter 2: Water
| LMMB 010 |
Standard Operating Procedure for Sample Collection of Atrazine
and Atrazine Metabolites (Eisenreich, S., Schottler, S., and Hines, N.) |
| LMMB 011 |
HOC Sampling Media Preparation and Handling; XAD-2 Resin and
GF/F Filters (Crecelius, E. and Lefkovitz, L.) |
| LMMB 012 |
Standard Operating Procedure for Site Selection and Sampling
for Mercury in Lakewater (Mason, R. and Sullivan, K.) |
| LMMB 013 |
Field Sampling Using the Rosette Sampler (Warren, G.) |
| LMMB 014 |
Standard Operating Procedure for the Sampling of
Particulate-Phase and Dissolved-Phase Organic Carbon in Great Lakes Waters (Grace
Analytical Lab) |
| LMMB 015 |
Standard Operating Procedure for Chlorophyll-a Sampling
Method: Field Procedure (Grace Analytical Lab) |
| LMMB 016 |
Standard Operating Procedure for Primary Productivity Using 14C:
Field Procedure (Grace Analytical Lab) |
| LMMB 017 |
USGS Field Operation Plan: Tributary Monitoring
(USGS/Eisenreich, S.) |
| LMMB 018 |
Trace Metal and Mercury Sampling Methods for Lake Michigan
Tributaries (Shafer, M.) |
Chapter 3: Sediment
| LMMB 019 |
Standard Operating Procedure for Collection of Sediment Samples
(Edgington, D. and Robbins, J.) |
| LMMB 020 |
Trap Sample Splitting (wet): Use of Sediment Traps for the Measurement of
Particle and Associated Contaminant Fluxes (Eadie, B.) |
Chapter 4: Plankton
| LMMB 021 |
Standard Operating Procedure for Sampling Lake Michigan Lower Pelagic
Foodchain for PCBs, Nonachlor, and Mercury (Swackhamer, D., Trowbridge, A., and Nater, E.) |
| LMMB 022 |
Sampling Procedure for Collection of Benthic Invertebrates for Contaminant
Analysis (Warren, G.) |
| LMMB023 |
Standard Operating Procedure for Phytoplankton Sample Collection and
Preservation (Grace Analytical Lab) |
| LMMB 024 |
Standard Operating Procedure for Zooplankton Sample Collection and
Preservation (Grace Analytical Lab) |
Chapter 5: Fish
| LMMB 025 |
Fish Processing Method (Hesselberg, R.) |
| LMMB 026 |
Quality Assurance Project Plan for Lake Trout and Forage Fish Sampling for
Diet Analysis and/or Contaminant Analysis (Brown, E. and Eck, G.) |
| LMMB 027 |
Quality Assurance Project Plan for Coho Sampling for Contaminant and Diet
Analysis (Holey, M. and Elliott, R.) |
(back to other methods)
Chapter 1: Organic Analysis
| LMMB 028 |
Instrumental Analysis and Quantitation of Polycyclic Aromatic
Hydrocarbons and Atrazine: IADN Project (Cortes, D. and Brubaker, W.) |
| LMMB 029 |
Analysis of PCBs and Pesticides in Air and Precipitation
Samples : IADN Project - Gas Chromatography Procedure (Basu, I.) |
| LMMB 030 |
Analysis of PCBs, Pesticides, and PAHs in Air and
Precipitation Samples: IADN Project - Sample Preparation Procedure (Basu, I.) |
| LMMB 031 |
Analysis of PCBs, Pesticides, and PAHs in Air and
Precipitation Samples: Sample Preparation Procedures (Harlin, K. and Surratt, K.) |
| LMMB 032 |
Standard Operating Procedure for the Analysis of PAHs and
Atrazine by GC/Ion Trap MS (Peters, C. and Harlin, K.) |
| LMMB 033 |
Standard Operating Procedure for the Analysis of PCBs and
Organochlorine Pesticides by GC-ECD (Harlin, K., Surratt, K., and Peters, C.)
Appendix C |
| LMMB 034 |
Standard Operating Procedure for Isolation, Extraction and
Analysis of Atrazine, DEA and DIA (Eisenreich, S., Schottler, S., and Hines, N.) |
| LMMB 035 |
Standard Operating Procedures for Semivolatile Organic
Compounds in Dry Deposition Samples (Eisenreich, S. and Franz, T.) |
| LMMB 036 |
Extraction and Cleanup of XAD-2 Resin Cartridges for
Polychlorinated Biphenyls and Trans-Nonachlor (Crecelius, E. and Lefkovitz, L.) |
| LMMB 037 |
Extraction and Cleanup of Glass Fiber Filters for
Polychlorinated Biphenyls and Trans-Nonachlor (Crecelius, E. and Lefkovitz, L.) |
| LMMB 038 |
PCB Congener Analysis of XAD-2 Resins and GFF Filters Using
GC/ECD (Crecelius, E. and Lefkovitz, L.) |
| LMMB 039 |
PCBs and Pesticides in Surface Water by XAD-2 Resin Extraction
(Wisconsin State Lab of Hygiene) |
| LMMB 040 |
Extraction and Cleanup of Sediments for Semivolatile Organics
Following the Internal Standard Method (Van Hoof, P. and Hsieh, J.) |
| LMMB 041 |
Analysis of Polychlorinated Biphenyls and Chlorinated
Pesticides by Gas Chromatography with Electron Capture Detection (Van Hoof, P. and Hsieh,
J.) |
| LMMB 042 |
Standard Operating Procedure for the Analysis of PCB Congeners
by GC/ECD and Trans-Nonachlor by GC/MS/ECNI (Swackhamer, D., Trowbridge, A., and Nater,
E.) |
| LMMB 043 |
Extraction and Lipid Separation of Fish Samples for
Contaminant Analysis and Lipid Determination (Schmidt, L.) |
| LMMB 044 |
Analysis of Total PCBs and PCB Congeners and Trans-nonachlor
in Fish by Gas Chromatography/Negative Chemical Ionization Single Ion Mass Spectrometry
(Schmidt, L.) |
Chapter 2: Mercury Analysis
| LMMB 045 |
Standard Operating Procedure for Analysis of Vapor Phase Mercury (Keeler,
G. and Landis, M.) |
| LMMB 046 |
Standard Operating Procedure for Analysis of Mercury in Precipitation
(Keeler, G. and Landis, M.) |
| LMMB 047 |
Standard Operating Procedure for Analysis of Particulate Phase Mercury
(Keeler, G. and Landis, M.) |
| LMMB 048 |
Standard Operating Procedure for Mercury Analysis (Mason, R. and Sullivan,
K.) |
| LMMB 049 |
Total Mercury Analysis in Aqueous Samples (Hurley, J.) |
| LMMB 050 |
Standard Operating Procedure for Analysis of Sediment for Total Mercury
Using the Cold Vapor Technique with the Leeman Labs, Inc. Automated Mercury System
(Uscinowicz, T. and Rossmann, R.) |
| LMMB 051 |
Mercury in Plankton (Nater, E. and Cook, B.) |
| LMMB 052 |
Versatile Combustion-Amalgamation Technique for the Photometric
Determination of Mercury in Fish and Environmental Samples (Willford, W., Hesselberg, R.,
and Bergman, H.) |
| LMMB 053 |
Analysis of Fish for Total Mercury (Nriagu, J.) |
NOTE: For “Standard Operating Procedure for Lab Analysis of Coho
Salmon Stomachs and Data Entry”, see Volume 1, Chapter 5, LMMB 026, Quality
Assurance Project Plan for Coho Sampling for Contaminant and Diet Analysis.
(back to other methods)
Chapter 1: Metals
| LMMB 054 |
Laboratory Methods for ICP-MS Analysis of Trace Metals in Precipitation
(Talbot, J. and Weiss, A.) |
| LMMB 055 |
Standard Operating Procedures for Preparation, Handling and Extraction of
Dry Deposition Plates: Dry Deposition of Atmospheric Particles (Paode, R. and Holsen, T.) |
| LMMB 056 |
Standard Operating Procedure for EPA’s LBL Energy Dispersive X-Ray
Fluorescence Spectrometry (Kellogg, R.) |
| LMMB 057 |
Analysis of Surface Waters for Trace Elements by Inductively-Coupled
Plasma Mass Spectrometry (Shafer, M. and Overdier, J.) |
Chapter 2: Conventionals
| LMMB 058 |
ESS Method 130.1: General Auto Analyzer Procedures (Wisconsin
State Lab of Hygiene) |
| LMMB 059 |
ESS Method 200.5: Determination of Inorganic Anions in Water
by Ion Chromatography (Wisconsin State Lab of Hygiene) |
| LMMB 060 |
ESS Method 140.4: Chloride - Automated Flow Injection Analysis
(Wisconsin State Lab of Hygiene) |
| LMMB 061 |
ESS Method 220.3: Ammonia Nitrogen and Nitrate + Nitrite
Nitrogen, Automated Flow Injection Analysis Method (Wisconsin State Lab of Hygiene) |
| LMMB 062 |
ESS Method 230.1: Total Phosphorus and Total Kjeldahl
Nitrogen, Semi-Automated Method (Wisconsin State Lab of Hygiene) |
| LMMB 063 |
ESS Method 310.1: Ortho-Phosphorus, Dissolved Automated,
Ascorbic Acid (Wisconsin State Lab of Hygiene) |
| LMMB 064 |
ESS Method 310.2: Phosphorus, Total, Low Level (Persulfate
Digestion) (Wisconsin State Lab of Hygiene) |
| LMMB 065 |
ESS Method 340.2: Total Suspended Solids, Mass Balance (Dried
at 103-105°C) Volatile Suspended Solids (Ignited at 550°C) (Wisconsin State Lab of
Hygiene) |
| LMMB 066 |
Outline of Standard Protocols for DOC Analyses (Shafer, M.) |
| LMMB 067 |
Outline of Standard Protocols for Particulate Organic Carbon
(POC) Analyses (Baldino, R.) |
| LMMB 068 |
ESS Method 360.2: Silica Dissolved, Automated, Colorimetric
(Wisconsin State Lab of Hygiene) |
| LMMB 069 |
ESS Method 360.3: Silica, Dissolved, Micro Level Automated,
Colorimetric (Wisconsin State Lab of Hygiene) |
| LMMB 070 |
ESS Method 370.2: Sulfates Colorimetric, Automated,
Methylthymol Blue (Wisconsin State Lab of Hygiene) |
| LMMB 071 |
ESS Method 370.3: Sulfates Colorimetric, Automated Flow
Injection, Methylthymol Blue (Wisconsin State Lab of Hygiene) |
| LMMB 072 |
Standard Operating Procedure for Chloride and Silica in Lake
Water (Lachat Method) (Grace Analytical Lab) |
| LMMB 073 |
Standard Operating Procedure for Dissolved Reactive
Phosphorous (Lachat Method) (Grace Analytical Lab) |
| LMMB 074 |
Standard Operating Procedure for Ammonia (Lachat Method)
(Grace Analytical Lab) |
| LMMB 075 |
Standard Operating Procedure for Nitrate, Nitrite (Lachat
Method) (Grace Analytical Lab) |
| LMMB 076 |
Standard Operating Procedure for Total Kjeldahl Nitrogen
(Lachat Method) (Grace Analytical Lab) |
| LMMB 077 |
Standard Operating Procedure for Total and Dissolved
Phosphorous (Lachat Method) (Grace Analytical Lab) |
| LMMB 078 |
Analysis of Total Suspended Particles (TSP) and Total Organic
Carbon (TOC) in Air Samples: Integrated Atmospheric Deposition Network (IADN) TSP/TOC
Procedure (Wassouf, M. and Basu, I.) |
| LMMB 079 |
Standard Operating Procedures for Determining Total
Phosphorus, Available Phosphorus, and Biogenic Silica Concentrations of Lake Michigan
Sediments and Sediment Trap Material (Johengen, T.) |
| LMMB 080 |
Standard Operating Procedure for Perkin Elmer CHN Analyzer
(Model 2400) (Eadie, B.) |
| LMMB 081 |
Quality Assurance Plan for the Use of Sediment Traps (Eadie,
B.) |
Chapter 3:Radiochemistry
| LMMB 082 |
Standard Operating Procedure for Primary Productivity Using 14C:
Laboratory Procedures (Grace Analytical Lab) |
| LMMB 083 |
LProtocol for Standard Analysis for Cesium-137 (Robbins, J. and Edgington,
D.) |
| LMMB 084 |
Determination of the Activity of Lead-210 in Sediments and Soils
(Edgington, D. and Robbins, J.) |
Chapter 4:Biomonitoring
| LMMB 085 |
Standard Operating Procedure for Chlorophyll-a and Pheophytin-a
(Turner Designs Method) (Grace Analytical Lab) |
| LMMB 086 |
ESS Method 150.1: Chlorophyll - Spectrophotometric (Wisconsin State Lab of
Hygiene) |
| LMMB 087 |
Standard Operating Procedure for Phytoplankton Analysis (Grace Analytical
Lab) |
| LMMB 088 |
Standard Operating Procedure for Zooplankton Analysis (Grace Analytical
Lab) |
| LMMB 089 |
Quality Assurance Project Plan: Diet Analysis for Forage Fish (Davis, B.
and Savino, J.) |
Chapter 5:Shipboard Measurements
| LMMB 090 |
Standard Operating Procedure for GLNPO Turbidity: Nephelometric Method
(Palmer, M.) |
| LMMB 091 |
Standard Operating Procedure for GLNPO Total Alkalinity Titration (Palmer,
M.) |
| LMMB 092 |
Standard Operating Procedure for Electrometric pH (Palmer, M.) |
| LMMB 093 |
Standard Operating Procedure for Meteorological Data Aboard the R/V Lake
Guardian (Palmer, M.) |
| LMMB 094 |
Standard Operating Procedure for GLNPO Specific Conductance: Conductivity
Bridge (Palmer, M.) |
| LMMB 095 |
Total Hardness Titration (Palmer, M.) |
| LMMB 096 |
Standard Operating Procedure for the Analysis of Dissolved-Phase Organic
Carbon in Great Lakes Waters (Grace Analytical Lab) |
| LMMB 097 |
Standard Operating Procedure for the Analysis of Particulate-Phase Organic
Carbon in Great Lakes Waters (Grace Analytical Lab) |
| LMMB 098 |
Standard Operating Procedure for the Sampling and Analysis of Total
Suspended Solids in Great Lakes Waters (Grace Analytical Lab) |
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